HRID1289435

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID79098

Tetrahydro-2,5-dimethoxy-furan

C6H12O3

结构：CCOP(=O)(OCC)C1CCc2c(N)c(C(F)(F)F)cc3[nH]c(=O)c(=O)n1c23

HCID23206547

未命名化合物

PRODUCTS

生成物

结构：CCOP(=O)(OCC)C1CCc2c(-n3cccc3)c(C(F)(F)F)cc3[nH]c(=O)c(=O)n1c23

HCID23206551

未命名化合物

PROCEDURE

实验过程

211 mg of 8-amino-9-trifluoromethyl-2,3-dioxo-1,2,3,5,6,7-hexahydro-pyrido[1,2,3-de]quinoxaline-5-phosphonic acid diethyl ester and 66 mg of 2,5-dimethoxytetrahydrofuran are reacted for one hour at 140° C. bath temperature. After recrystallization from ethanol, 123 mg of 8-(1-pyrrolyl)-9-trifluoromethyl-2,3-dioxo-1,2,3,5,6,7-hexahydro-pyrido[1,2,3-de]quinoxaline-5-phosphonic acid diethyl ester of melting point 268° C. is obtained.

WORKUP

后处理

customAfter recrystallization from ethanol, 123 mg of 8-(1-pyrrolyl)-9-trifluoromethyl-2,3-dioxo-1,2,3,5,6,7-hexahydro-pyrido[1,2,3-de]quinoxaline-5-phosphonic acid diethyl ester of melting point 268° C.
customis obtained