HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylmethyl 4-(2,3-dihydro-1H-inden-2-yl)-2-butenoate → HCID 10465518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylmethyl 4-(2,3-dihydro-1H-inden-2-yl)-2-butenoate | HCID 54078263 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10465518 | HCID 10465518 | 85.1% |
Reaction Steps
Dissovled in 120 ml of methanol were 6.45 g (22.1 mmol) of benzyl-4-(indan-2-yl)-2-butenoate, and 0.6 g of 10% palladium-carbon was added to the solution, followed by vigorous stirring for 2.5 hours under a hydrogen atmosphere. The catalyst was separated by filtration, and the filtrate was concentrated to obtain 3.84 g of 4-(indan-2-yl)butanoic acid as a crystal. Yield: 85%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750524 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-d6a1fa13c10e41628c1ab483f2ec156e |
| Source note | uspto-grants-1998_05 |