HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 69954406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | 5,6-Dimethyl-2-chloro4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)pyrimidine | HCID 11185318 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69954406 | HCID 69954406 | 9.6% |
Reaction Steps
After N-methylaniline(1.5 ml, 14 mmol) was added to a mixture solution of 5,6-dimethyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(1.9 g, 6.6 mmol) and dimethylformamide(10 ml), 0.25 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-135df7fa8c3349c89e21b1353730c120 |
| Source note | uspto-grants-1998_05 |