HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-1,2,3,4-tetrahydroisoquinoline → HCID 18921790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-1,2,3,4-tetrahydroisoquinoline | HCID 92214 | — |
| Reactant | HCID 18921712 | HCID 18921712 | — |
| Product | HCID 18921790 | HCID 18921790 | 56.7% |
Reaction Steps
In accordance with the same procedure as in Step 1 of Example 1, except that 1-methyl-1,2,3,4-tetrahydroisoquinoline (2.3 g, 15.6 mmol) and 2,4-dichloro-5-methyl-6-ethylpyrimidine (2.7 g, 14.1 mmol) prepared in Preparation 4 were used as starting materials, 2.3 g of the titled compound was prepared. (Yield: 54%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-0d74cf8bf5474b829d525eb5bd1c2b44 |
| Source note | uspto-grants-1998_05 |