HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 18921704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Reactant | HCID 18921790 | HCID 18921790 | — |
| Product | HCID 18921704 | HCID 18921704 | 22.1% |
Reaction Steps
After 4-fluoro-2-methylaniline(0.55 ml, 4.95 mmol) was added to a mixture solution of 5-methyl-6-ethyl-4-(1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(0.80 g, 2.65 mmol) and dimethylformamide (5 ml), 0.25 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-9acd0d6f1f5e45d4bd0bfe1472f1211f |
| Source note | uspto-grants-1998_05 |