HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 69956318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921711 | HCID 18921711 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69956318 | HCID 69956318 | 26% |
Reaction Steps
After N-methylaniline(0.50 ml, 4.8 mmol) was added to a mixture solution of 4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloro-5,6,7,8-tetrahydroquinazoline(0.75 g, 2.40 mmol) and dimethylformamide(5 ml), 0.26 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-4117309df4bb4d5f8c29afa70b5630eb |
| Source note | uspto-grants-1998_05 |