HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methylaniline → HCID 18921767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Reactant | HCID 86752540 | HCID 86752540 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921767 | HCID 18921767 | 75.6% |
Reaction Steps
After 4-fluoro-2-methylaniline(0.25 ml, 2.20 mmol) was added to a mixture solution of 4-(1,2,3,4-tetrahydroisoquinolin-2-yl)-4-chlorocyclopenta[d]pyrimidine(0.58 g, 2.0 mmol) and dimethylformamide(5 ml), 0.34 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-520c004ba9474f7b8435c5a5c63fa2a7 |
| Source note | uspto-grants-1998_05 |