HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylpyrimidine → HCID 18921666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylpyrimidine | HCID 79471 | — |
| Reactant | 7-Methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine | HCID 14548169 | — |
| Product | HCID 18921666 | HCID 18921666 | 41.4% |
Reaction Steps
In accordance with the same procedure as in Step 1 of Example 1, except that 2,4-dichloro-6-methylpyrimidine(3.1 g, 19 mmol) and 7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine (2.9 g, 19 mmol) in Preparation 1 were used as starting materials, 2.2 g of the titled compound was obtained as white crystal. (Yield: 41%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-c5300c6cd8394a5085b4d09e92e796fc |
| Source note | uspto-grants-1998_05 |