HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methylaniline → HCID 18921708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Reactant | HCID 18921666 | HCID 18921666 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921708 | HCID 18921708 | 44.5% |
Reaction Steps
After 4-fluoro-2-methylaniline(0.5 ml, 4.6 mmol) was added to a mixture solution of 6-methyl-4-(7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridin-6-yl)-2-chloropyrimidine(0.7 g, 2.5 mmol) and dimethylformamide(10 ml), 0.45 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-af372a933bcc4d7e816edeb8f3112688 |
| Source note | uspto-grants-1998_05 |