HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 17890624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921666 | HCID 18921666 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 17890624 | HCID 17890624 | 49.8% |
Reaction Steps
After N-methylaniline(0.45 ml, 4.05 mmol) was added to a mixture solution of 6-methyl-4-(7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridin-6-yl)-2-chloropyrimidine(0.75 g, 2.7 mmol) and dimethylformamide(10 ml), 0.52 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-abb1f5b52ef84329976afb1f37ec3e92 |
| Source note | uspto-grants-1998_05 |