HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-5,6-dimethylpyrimidine → HCID 18921690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-5,6-dimethylpyrimidine | HCID 241553 | — |
| Reactant | 7-Methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine | HCID 14548169 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921690 | HCID 18921690 | 39.4% |
Reaction Steps
In accordance with the same procedure as in Step 1 of Example 1, except that N,N-dimethylformamide(20 ml), 5,6-dimethyl-2,4-dichloropyrimidine(2.8 g, 16 mmol) prepared in Step 1 of Example 12 and 7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine (2.7 g, 17.6 mmol) in Preparation 2 were used as starting materials, 1.85 g of the titled compound was prepared. (Yield: 39.4%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-6401f60c38ed4791ad2735fa0f848147 |
| Source note | uspto-grants-1998_05 |