Triethylamine → HCID 18921720, compound

Participants

Reaction Steps

In accordance with the same procedure as in Step 1 of Example 1, except that triethylamine(2.2 ml), N,N-dimethyl formamide(20 ml), 2,4-dichloro-5-methyl-6-ethylpyrimidine (2.7 g, 14.1 mmol) prepared in Preparation 4 and 7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine(2.4 g, 15.7 mmol) prepared in Preparation 1 were used as starting materials, 2.23 g of the titled compound was prepared. (Yield: 51.3%)

Provenance & Evidence