HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 18921763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | HCID 18921804 | HCID 18921804 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921763 | HCID 18921763 | 78.3% |
Reaction Steps
After 4-fluoroaniline(0.30 ml, 3.17 mmol) was added to a mixture solution of 6-ethyl-2-(1,2,3,4-tetrahydroisoquinolin-2-yl)-4-chloropyrimidine(0.40 g, 1.46 mmol) and dimethylformamide(10 ml), 0.44 g of the titled compound was obtained in accordance with the same procedure as in Step 4 of Example 57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-db15717570b34134b53e3fd24a8ea015 |
| Source note | uspto-grants-1998_05 |