HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 67627202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921804 | HCID 18921804 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67627202 | HCID 67627202 | 13.2% |
Reaction Steps
After N-methylaniline(0.10 ml, 9.22 mmol) was added to a mixture solution of 6-ethyl-2-(1,2,3,4-tetrahydroisoquinolin-2-yl)-4-chloropyrimidine(1.20 g, 4.38 mmol) and dimethylformamide(10 ml), 0.22 g of the titled compound was obtained in accordance with the same procedure as in Step 4 of Example 57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-713a17f53c89418f99acb7603a6706e9 |
| Source note | uspto-grants-1998_05 |