HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 178506581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | Methanesulfonate | HCID 85257 | — |
| Product | HCID 178506581 | HCID 178506581 | — |
Reaction Steps
Add 30 gms. of the mesylate prepared in step (a) to 300 ml. methylethyl ketone (MEK), then add 90 gm. sodium iodide and reflux for about 30 minutes. Remove the solvent and extract with methylene chloride to yield trans 1,4-bis iodomethyl cyclohexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750532 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-b9c0f1cfe03e45848f9b3839cb6c9472 |
| Source note | uspto-grants-1998_05 |