HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-1,6-dimethylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-6-methylpyridine | HCID 19075369 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(3-Hexylthio-1,2,5-thiadiazol-4-yl)-1,6-dimethylpyridinium iodide | HCID 19075328 | — |
Reaction Steps
Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-hexylthio-1,2,5-thiadiazol-4-yl)-6-methylpyridine (4 mmol) in acetone (5 ml) and the reaction mixture was stirred at room temperature for 20 h. Evaporation of the reaction mixture gave the crude product, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750541 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-051fa5fa7abd4d43bcf6e89a5d8b6320 |
| Source note | uspto-grants-1998_05 |