Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 4-Chlorobenzohydrazide | HCID 10816 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178485225 | HCID 178485225 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178513170 | HCID 178513170 | 104.7% |
Reaction Steps
The synthesis was carried out according to the method of Example 1-(1). 4-Chlorobenzoic acid hydrazide (34.8 g), methylisothiourea sulfate (115.4 g), sodium hydroxide (17.1 g), water (440 ml) and methanol (700 ml) were used as reagents. The mixture was stirred for 4 days at 60° C. to give 45.4 g of a pale-brown solid which was a mixture of a hydrazide compound and the objective compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05750545 |
|---|
| Source dataset | uspto-grants-1998_05 |
|---|
| ORD ID | ord-3d761e524d6a482c880699c727a262cb |
|---|
| Source note | uspto-grants-1998_05 |
|---|
