HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → 3-Amino-5-(4-chloro-1-naphthyl)-1H-1,2,4-triazol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 1-Naphthalenecarboxylic acid, 4-chloro-, methyl ester | HCID 22261615 | — |
| Reactant | HCID 178513186 | HCID 178513186 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Amino-5-(4-chloro-1-naphthyl)-1H-1,2,4-triazol | HCID 10752854 | — |
Reaction Steps
The synthesis method of Example 7-(2) was applied. The compound (1.90 g) obtained in (3) above, methanol (20 ml), metallic sodium (810 mg) and aminoguanidine nitrate (4.8 g) were used as reagents to give a brown solid (2.27 g). The obtained compound was used as it was in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-8a69dfb4bb214ae4bba3778604442fac |
| Source note | uspto-grants-1998_05 |