huagongshe.com
HRID1289774

反应详情

EQUATION

反应方程式

HRID 1289774 的结构方程式

REACTANTS

反应物

2
结构：CN=C=S
HCID11167

Methyl isothiocyanate

C2H3NS

结构：Cc1nc(N)n[nH]1
HCID234610

5-methyl-4H-1,2,4-triazol-3-amine

C3H6N4

PRODUCTS

生成物

1
结构：CNC(=S)n1nc(C)nc1N
HCID10702319

未命名化合物

收率 29%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The synthesis method of Example 1-(3) was applied. The compound (664 mg) obtained in (2) above, dimethylformamide (13 ml) and methyl isothiocyanate (600 mg) were used as reagents to give 340 mg of white crystals (yield 29%).