Methyl isothiocyanate → HCID 10702319, compound

HRID 1289774Notes

Reaction equation

HRID 1289774 reaction equation
[NH2:1][C:2]1[N:6]=[C:5]([CH3:7])[NH:4][N:3]=1.[CH3:8][N:9]=[C:10]=[S:11]>CN(C)C=O>[NH2:1][C:2]1[N:3]([C:10]([NH:9][CH3:8])=[S:11])[N:4]=[C:5]([CH3:7])[N:6]=1

Participants

4

Reactant 2

HCID 11167Methyl isothiocyanateHCID 2346103-Amino-5-methyl-4H-1,2,4-triazole

Product 1

HCID 10702319HCID 10702319, compoundYield 29%

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The synthesis method of Example 1-(3) was applied. The compound (664 mg) obtained in (2) above, dimethylformamide (13 ml) and methyl isothiocyanate (600 mg) were used as reagents to give 340 mg of white crystals (yield 29%).

Sources & evidence

ORD record
ord-49a7c28491a444d1a3f480263c3ca0df
Source dataset
uspto-grants-1998_05
Patent number
US05750545

Reaction notes

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