HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 10725863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | 3,5-Diamino-1,2,4-triazole | HCID 15078 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 10725863 | HCID 10725863 | 68% |
Reaction Steps
The synthesis method of Example 1-(3) was applied. 3,5-Diamino-1H-1,2,4-triazole (11.0 g), dimethylformamide (100 ml) and methyl isothiocyanate (10.0 g) were used as reagents. After the reaction, recrystallization from ethyl acetate gave 13.0 g of white powdery crystals (yield (68%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-f71d34baffd24603867bf57e1aef3afa |
| Source note | uspto-grants-1998_05 |