Dimethylformamide → HCID 10725863, compound

HRID 1289775Notes

Reaction equation

HRID 1289775 reaction equation
[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[NH:4][N:3]=1.CN(C)C=O.[CH3:13][N:14]=[C:15]=[S:16]>C(OCC)(=O)C>[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[N:4]([C:15]([NH:14][CH3:13])=[S:16])[N:3]=1

Participants

5

Reactant 3

HCID 6228DimethylformamideHCID 11167Methyl isothiocyanateHCID 150783,5-Diamino-1,2,4-triazole

Product 1

HCID 10725863HCID 10725863, compoundYield 68%

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The synthesis method of Example 1-(3) was applied. 3,5-Diamino-1H-1,2,4-triazole (11.0 g), dimethylformamide (100 ml) and methyl isothiocyanate (10.0 g) were used as reagents. After the reaction, recrystallization from ethyl acetate gave 13.0 g of white powdery crystals (yield (68%).

Sources & evidence

ORD record
ord-f71d34baffd24603867bf57e1aef3afa
Source dataset
uspto-grants-1998_05
Patent number
US05750545

Reaction notes

Loading…