HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → Phenylpropynoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Phenylpropiolic Acid | HCID 69475 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Phenylpropynoic acid methyl ester | HCID 138378 | — |
Reaction Steps
The synthesis method of Example 7-(1) was applied. Phenylpropiolic acid (5.16 g), : 1,2-dichloroethane (40 ml), methanol (5 ml) and concentrated sulfuric acid (0.2 ml) were used as reagents to quantitatively give a colorless transparent liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-f0547759d04a4c568d460899e2bc80dc |
| Source note | uspto-grants-1998_05 |