HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylpropynoic acid methyl ester → HCID 10655081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylpropynoic acid methyl ester | HCID 138378 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 178418668 | HCID 178418668 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10655081 | HCID 10655081 | 75% |
Reaction Steps
The synthesis method of Example 7-(2) was applied. The compound (5.63 g) obtained in (1) above, methanol (85 ml), metallic sodium (3.29 g) and aminoguanidine hydrochloride (15.8 g) were used as reagents to give 4.87 g of a pale-brown solid (yield 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-c3b85abe699c4f6abb8e7fecf294166a |
| Source note | uspto-grants-1998_05 |