HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → 5-Hydroxypentyl isothiocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | 5-Aminopentan-1-ol | HCID 75634 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 5-Hydroxypentyl isothiocyanate | HCID 10486981 | — |
Reaction Steps
The synthesis method of Example 45-(1) was applied. 5-Hydroxypentylamine (6.00 g), carbon disulfide (40 ml), triethylamine (8.3 ml), ethyl chlorocarbonate (5.4 ml), triethylamine (8.3 ml) and chloroform (20 ml) were used as reagents. After the reaction, a yellow liquid was quantitatively obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-8df58fab982b4bcdb01a58c3cde4623e |
| Source note | uspto-grants-1998_05 |