HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 10513597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 5-Hydroxypentyl isothiocyanate | HCID 10486981 | — |
| Reactant | HCID 178418311 | HCID 178418311 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10513597 | HCID 10513597 | 19% |
Reaction Steps
The synthesis method of Example 1-(3) was applied. 3-Amino-1H-1,2,4-triazole (4.00 g), dimethylformamide (25 ml) and 5-hydroxypentyl isothiocyanate (9.24 g) were used as reagents. After the reaction, silica gel column chromatography (chloroform-methanol) was applied to give 2.06 g of white crystals (yield 19%). The crystals were subjected to recrystallization from chloroform to give white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-a324b6d0dd5c453fb78dcb3aa5713fed |
| Source note | uspto-grants-1998_05 |