HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol, 1,1-diethoxy-, 1-acetate → 2-[(Dimethylaminomethylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7(6H)-thione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol, 1,1-diethoxy-, 1-acetate | HCID 84166 | — |
| Reactant | 5-Amino-3-[(dimethylaminomethylidene)amino]-1-[methylamino(thiocarbonyl)]-1H-1,2,4-triazole | HCID 86752544 | — |
| Product | 2-[(Dimethylaminomethylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7(6H)-thione | HCID 86752546 | 56% |
Reaction Steps
The synthesis method of Example 55 was applied. The compound (486 mg) obtained in Example 33 and diethoxymethyl acetate (5 ml) were used as reagents. The mixture was reacted at 95° C. for 2 hours to give 282 mg of pale-brown crystals (yield 56%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-691622487f6947b78fa0f9de9897e094 |
| Source note | uspto-grants-1998_05 |