HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol, 1,1-diethoxy-, 1-acetate → 2-[(N-Benzylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7 (6H)-thione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol, 1,1-diethoxy-, 1-acetate | HCID 84166 | — |
| Reactant | 5-Amino-3-[(N-benzylidene)amino]-1-[methylamino(thiocarbonyl)]-1H-1,2,4-triazole | HCID 44332154 | — |
| Product | 2-[(N-Benzylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7 (6H)-thione | HCID 86752548 | 93% |
Reaction Steps
The synthesis method of Example 55 was applied. The compound (783 mg) obtained in Example 37 and diethoxymethyl acetate (5 ml) were used as reagents. The mixture was reacted at 90° C. for 1.5 hours to give 757 mg of white powdery crystals (yield 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-a8810adf3fba431d9f89cfd75ccdfe35 |
| Source note | uspto-grants-1998_05 |