HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol, 1,1-diethoxy-, 1-acetate → HCID 18922213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol, 1,1-diethoxy-, 1-acetate | HCID 84166 | — |
| Reactant | HCID 18922220 | HCID 18922220 | — |
| Product | HCID 18922213 | HCID 18922213 | 71.5% |
Reaction Steps
The synthesis method of Example 55 was applied. The compound (280 mg) obtained in Example 44 and diethoxymethyl acetate (6.0 g) were used as reagents. The mixture was reacted at 100° C. for 2.5 hours to give 207 mg of white crystals (yield 71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-525a34ba25ce46a1902249b40b83d708 |
| Source note | uspto-grants-1998_05 |