HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11132869, compound → HCID 11025076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11132869 | HCID 11132869 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 11025076 | HCID 11025076 | 174.1% |
Reaction Steps
1.0 g of N-(1-t-butoxycarbonylpiperidin-4-yl)-2-cyclobutyl-2-hydroxy-2-phenylacetamide was dissolved in 25 ml of a 4N hydrochloric acid solution in dioxane, and this solution was stirred at room temperature overnight. Then, the reaction mixture was evaporated to dryness under reduced pressure to obtain 0.83 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750540 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-7f263680a5fb4d00a3e1cd1391766b89 |
| Source note | uspto-grants-1998_05 |