HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69832107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 69832108 | HCID 69832108 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69832107 | HCID 69832107 | — |
Reaction Steps
(2R)-N-[1-(Cycloheptylmethyl)piperidin-4-yl]-2-cyclopentyl-2-hydroxy-2-phenylacetamide obtained in Example 34 was dissolved in chloroform and a 4N hydrochloric acid solution in ethyl acetate was added thereto. The solvent was distilled off under reduced pressure and the residue was washed with diethyl ether. The resulting solid was recrystallized from ethanol-diethyl ether to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750540 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-2b9a43ff30f74f9ea109f87f80cdff6a |
| Source note | uspto-grants-1998_05 |