HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 22885701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 22885700 | HCID 22885700 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22885701 | HCID 22885701 | — |
Reaction Steps
The residue from Step B was taken up in methylene chloride and a trace of DMF was added followed by 0.21 mL of oxalyl chloride. The reaction was stirred at room temperature for 1 h and then evaporated and used in Step D.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750549 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-95ddcc31c776468381f1bf0326c3a2c6 |
| Source note | uspto-grants-1998_05 |