Hydrochloric Acid → HCID 67669777, compound

Participants

Reaction Steps

Exposure of the product from Step A above to 1.0 equivalent of HCl in methanol/ethyl ether followed by evaporation provided the title compound. NMR (400 MHz, CD3OD): δ 7.43-7.37 (m, 3H), 7.26-7.19 (m, 3H), 7.14 (d, 1H, J=9 Hz), 4.25 (d, 1H, J=13 Hz), 4.10 (d, 1H, J=13 Hz), 3.95-3.85 (m, 2H), 3.74 (s, 3H), 3.63 (s, 3H), 3.37 (quartet, 1H, J=9 Hz), 2.48-2.38 (m, 2H), 2.36 (s, 3H), 2.20 (s, 3H), 2.16-1.96 (m, 2H).

Provenance & Evidence