HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → (R)-3-(3,4-Dihydroxyphenyl)-2-propylamine hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3,4-Dma hydrochloride, (R)- | HCID 15556607 | — |
| Product | (R)-3-(3,4-Dihydroxyphenyl)-2-propylamine hydrobromide | HCID 67643451 | — |
Reaction Steps
A solution of (R)-3-(3,4-dimethoxyphenyl)-2-propylamine hydrochloride (500 mg, 2.15 mMol) in hydrogen bromide (48%, 5 ml) was stirred at 100° C. under an argon atmosphere for 20 hours. After cooling, the solvent was evaporated and the residue was dried giving the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750701 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-48f7db6293ca45a6bf7fec2b5b5d0968 |
| Source note | uspto-grants-1998_05 |