HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Acid → HCID 178485754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 178485751 | HCID 178485751 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178485754 | HCID 178485754 | 79.8% |
Reaction Steps
The compound (778 mg) obtained in Example 1 was dissolved in ethyl acetate (10 ml) and a solution of maleic acid (132 mg) in ethyl acetate (15.5 ml) and ethanol (1.55 ml) was dropwise added. After stirring overnight at room temperature, crystals were collected by filtration and dried under reduced pressure to give 723 mg of the title compound as white crystals (see Table 17).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750696 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-902c1afeed5b40b48f9435e57e378e33 |
| Source note | uspto-grants-1998_05 |