Dimethyl Carbonate → HCID 18413646, compound

Participants

Reaction Conditions

Reaction Steps

2.0 g of potassium hydroxide and 50 g of dimethyl carbonate were added to 108.0 g (1.00 mol) of 3-fluoro-1,2-butanediol, and the resulting mixture was stirred at 60° C. for 12 hours. After filtering off potassium hydroxide, the mixture was distilled to obtain 101.2 g of 4-(1-fluoroethyl) -1,3-dioxolan-2-one (yield 75.5%). An elemental analysis was performed and the following values were observed:

Provenance & Evidence