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HRID129032

反应详情

EQUATION

反应方程式

HRID 129032 的结构方程式

REACTANTS

反应物

2
结构：CC(C)=CCCC(C)=CCCC(C)=CCO
HCID3327

Farnesol

C15H26O

结构：O=C(Cl)Cc1ccccc1
HCID7679

Benzeneacetyl chloride

C8H7ClO

PRODUCTS

生成物

1
结构：CC(C)=CCCC(C)=CCCC(C)=CCOC(=O)Cc1ccccc1
HCID54216610

未命名化合物

收率 54%

PROCEDURE

实验过程

A mixture of farnesol (440 mg, 2 mmol) and phenylacetyl chloride (584 mg, 7.8 mmol) was refluxed for 2.5 hours. Extraction with hexane, and purification yielded 368 mg (yield: 54%) of oil having the following physical properties.

WORKUP

后处理

  1. temperaturewas refluxed for 2.5 hours
  2. extractionExtraction
  3. customwith hexane, and purification