HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Amino-2,4,6-triiodo-1,3-benzenedicarboxylic acid → 5-Amino-2,4,6-triiodoisophthaloyl dichloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Amino-2,4,6-triiodo-1,3-benzenedicarboxylic acid | HCID 3015783 | — |
| Reactant | 1H-Imidazolium, 2-chloro-4,5-dihydro-1,3-dimethyl-, chloride | HCID 10986715 | — |
| Product | 5-Amino-2,4,6-triiodoisophthaloyl dichloride | HCID 9894858 | 93% |
Reaction Steps
The same procedures as described in Example 7 were carried out except that the reaction of 5-amino-2,4,6-triiodoisophthalic acid and 2-chloro-1,3-dimethylimidazolinium chloride was carried out at 90°-95° C. for 6 hours. 5-Amino-2,4,6-triiodoisophthaloyl dichloride thus obtained was 5.53 g (93% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750779 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-fa1f98ffe32d420985bc86a50f3d66b5 |
| Source note | uspto-grants-1998_05 |