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HRID1290361

反应详情

EQUATION

反应方程式

HRID 1290361 的结构方程式

REACTANTS

反应物

3
结构：Oc1ccc(F)cc1
HCID9732

4-Fluorophenol

C6H5FO

结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CC(=O)S[C@@H]1CO[C@@H](COS(=O)(=O)C(F)(F)F)C1
HCID86750748

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)S[C@@H]1CO[C@@H](COc2ccc(F)cc2)C1
HCID86750320

未命名化合物

收率 73.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 23 using 1.49 g of product from Example 22 in 1 ml of methylene chloride, 0.542 g of 4-fluorophenol, 2.5 ml of Hunig's base and 3 ml of methylene chloride to give 0.963 g of the desired compound.