HRID1290380

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID21912024

未命名化合物

HCID23694274

Sodium methanolate methanol

C2H7NaO2

结构：CC(=O)S[C@@H]1CO[C@@H](CN(OCc2ccccc2)C(C)=O)C1

HCID86750754

未命名化合物

PRODUCTS

生成物

结构：CC(=O)N(C[C@H]1C[C@H](S)CO1)OCc1ccccc1

HCID86750753

未命名化合物

收率 60.4%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 16 using 0.390 g of product from Example 72, 0.580 ml of 25% sodium methoxide/methyl alcohol, 0.850 ml of tetrahydrofuran and 1.26 ml of 2N hydrochloric acid/isopropyl alcohol to give 0.205 g of the desired product.