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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1290391Generated: November 3, 2026

Water → HCID 86752476, compound

https://huagongshe.com/reaction/1290391

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 86752478HCID 86752478—
CatalystPalladiumHCID 23938—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86752476HCID 86752476130.7%

Reaction Steps

The title compound is prepared by the procedure of Example 18 using 0.150 g of product from Example 95, 0.025 g of sodium bicarbonate, 3 ml of water, 9 ml of dioxane and 0.030 g of 10% palladium/carbon to give 0.0786 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05750735
Source datasetuspto-grants-1998_05
ORD IDord-1eae863e9f304242bc6f04075245a755
Source noteuspto-grants-1998_05