HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18916048, compound → HCID 15801175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18916048 | HCID 18916048 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15801175 | HCID 15801175 | — |
Reaction Steps
5.3 g (0.034 mole) of 5,6-dimethylquinoxaline were dissolved in 200 ml of ethanol and, after the addition of 1 g of Raney nickel, the resulting solution was hydrogenated for 2 h at room temperature/normal pressure. After filtration, the product was concentrated to dryness and recrystallized from methyl-t-butyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05752984 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-09be8a0ace6149278325e87c03570c4b |
| Source note | uspto-grants-1998_05 |