HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1-Adamantyl)-4-methoxybenzoyl chloride → Allyl 4-[3-(1-adamantyl)-4-methoxybenzamido]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1-Adamantyl)-4-methoxybenzoyl chloride | HCID 10804497 | — |
| Reactant | Prop-2-en-1-yl 4-aminobenzoate | HCID 13075143 | — |
| Product | Allyl 4-[3-(1-adamantyl)-4-methoxybenzamido]benzoate | HCID 67590904 | — |
Reaction Steps
In a manner analogous to Example 1(a) starting with 12.6 g (71 mmoles) of allyl 4-aminobenzoate and 21.6 g (71 mmoles) of 3-(1-adamantyl)-4-methoxy benzoyl chloride, 32 g of the expected amide whose melting point is 191°-192° C. are isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753239 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-0d96556a6778431daa5e51b8438ee45e |
| Source note | uspto-grants-1998_05 |