HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(11-(Carbomethoxy)undecanoyl)-N-Methyl-2-Benzyloxyaniline → N-(11-(Carbomethoxy)undecanoyl)-N-Methyl-2-Hydroxy aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(11-(Carbomethoxy)undecanoyl)-N-Methyl-2-Benzyloxyaniline | HCID 18795814 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-(11-(Carbomethoxy)undecanoyl)-N-Methyl-2-Hydroxy aniline | HCID 54429764 | — |
Reaction Steps
A solution of (28) (0.11 g., 0.25 mM) in methanol (11 mL) containing 10% palladium on carbon (30 mg.) is shaken in a 40 p.s.i. hydrogen atmosphere until no (V) remained (TLC analysis). The filtered solution was then concentrated in vacuo to give the title compound (29), used immediately in step P.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753641 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-bc99331d44024f0cae01331fc3717e18 |
| Source note | uspto-grants-1998_05 |