HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 18919352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 18919358 | HCID 18919358 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 18919352 | HCID 18919352 | — |
Reaction Steps
A mixture of 7-(1-methylethyl)-1,2,4-triazolo[1,5-a]pyrimidine (4.18 g), N-bromosuccinimide (4.59 g), and dibenzoylperoxide (70 mg) in tetrachloromethane (105 ml) was stirred and heated under reflux for 11 hours. The mixture was filtered and the solvent was removed from the filtrate to give 7-(1-bromo-1-methylethyl)-1,2,4-triazolo[1,5-a]pyrimidine. Yield 2.94 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753665 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-1c4f9d5e78e549ba84796dfdf75a3dc4 |
| Source note | uspto-grants-1998_05 |