HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2-(Propan-2-ylamino)phenyl]methanol → 2-((Propan-2-yl)amino)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2-(Propan-2-ylamino)phenyl]methanol | HCID 10797123 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-((Propan-2-yl)amino)benzaldehyde | HCID 11041035 | — |
Reaction Steps
While heating a solution of 40 g of 2-isopropylaminobenzyl alcohol in 200 ml toluene at 100° C., 58 g in total of activated manganese dioxide was added several times to the solution. After stirring at the same temperature for 30 minutes, insoluble matters were filtered off. The solvent was distilled off to give 2-isopropylaminobenzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753673 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-ce8f4cd759ae4e4f8d0ca8c3982018e6 |
| Source note | uspto-grants-1998_05 |