HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → [1,1'-Biphenyl]-2-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | o-Phenylbenzoic acid | HCID 70357 | — |
| Product | [1,1'-Biphenyl]-2-carbonyl chloride | HCID 12563768 | — |
Reaction Steps
A mixture of 5.6 g of 2-biphenylcarboxylic acid and 29 ml of thionyl chloride is heated on a steam bath for 0.5 hour and the volatiles removed under vacuum. Toluene (40 ml) is added (twice) and the solvent removed under vacuum to give 6.8 g of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753648 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-77025c080264465d82de5d6012beadb7 |
| Source note | uspto-grants-1998_05 |