HRID1290938

反应详情

EQUATION

反应方程式

HRID 1290938 的结构方程式

PROCEDURE

实验过程

A mixture of 2.0 g of 4-[[2-(phenylmethyl)benzoyl]amino]benzoic acid in 2.0 ml of thionyl chloride is heated on a steam bath for 1 hour. The volatiles are evaporated in vacuo to give 1.53 g of the desired product as an oil. M+ =346 as methyl ester.

WORKUP

后处理

  1. temperatureis heated on a steam bath for 1 hour
  2. customThe volatiles are evaporated in vacuo