HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-[[2-(Phenylmethyl)benzoyl]amino]benzoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-[[2-(Phenylmethyl)benzoyl]amino]benzoic Acid | HCID 22099697 | — |
| Product | 4-[[2-(Phenylmethyl)benzoyl]amino]benzoyl Chloride | HCID 22099663 | — |
Reaction Steps
A mixture of 2.0 g of 4-[[2-(phenylmethyl)benzoyl]amino]benzoic acid in 2.0 ml of thionyl chloride is heated on a steam bath for 1 hour. The volatiles are evaporated in vacuo to give 1.53 g of the desired product as an oil. M+ =346 as methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753648 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-c93354e0fe2d4f4ab1eb8ee041c31ab4 |
| Source note | uspto-grants-1998_05 |