Hydrochloric Acid → HCID 86752582, compound

HRID 1291037Notes

Reaction equation

HRID 1291037 reaction equation
[NH2:1][C:2]([NH2:22])=[N:3][C:4](=[O:21])[C:5]1[CH:6]([CH3:20])[C:7](=[S:17](=[O:19])=[O:18])[C:8]([N:12]2[CH:16]=[CH:15][N:14]=[CH:13]2)=[C:9]([CH3:11])[CH:10]=1.[ClH:23]>>[ClH:23].[ClH:23].[NH2:22][C:2]([NH2:1])=[N:3][C:4](=[O:21])[C:5]1[CH:6]([CH3:20])[C:7](=[S:17](=[O:19])=[O:18])[C:8]([N:12]2[CH:16]=[CH:15][N:14]=[CH:13]2)=[C:9]([CH3:11])[CH:10]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86752580HCID 86752580, compound

Product 1

HCID 86752582HCID 86752582, compound

Procedure

4 g of N-diaminomethylene-2-methyl-4-(1-imidazolyl)-5-methylsulfonylbenzamide [obtainable according to Example 1] are treated with 1-molar aqueous HCl solution for 1 hour and then freeze-dried. N-Diaminomethylene-2-methyl-4-(1-imidazolyl)-5-methyl-sulfonylbenzamide dihydrochloride is obtained.

Workup

  1. customfreeze-dried

Sources & evidence

ORD record
ord-2f57cb825c8c4ec79110c09487aa3ba3
Source dataset
uspto-grants-1998_05
Patent number
US05753680

Reaction notes

Loading…