HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18919805, compound → HCID 18919804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18919805 | HCID 18919805 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18919804 | HCID 18919804 | 185.9% |
Reaction Steps
0.155 g (0.00047 mol) of 1-(2-chloro-benzyl)-piperidin-4-yl benzoate was dissolved in 14 ml of ether, filtered, diluted with 0.4 ml of methanol and treated with 4.7 ml of 1N ethereal HCI. The separated precipitate was filtered off and dried. 0.16 g (93%) of 1-(2-chloro-benzyl)-piperidin-4-yl benzoate hydrochloride (1:1) was obtained as white crystals;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753679 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-bac220263ad64071ad4ddcd9172284c3 |
| Source note | uspto-grants-1998_05 |